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href=\"\u002Fen\u002Fcas\u002F65-49-6_1150743.html#duXinDiv\">对氨基水杨酸毒性英文版\u003C\u002Fa>\u003C\u002Fp>\n\n\u003C\u002Ftd>","\u003Cp>1.由间氨基酚经羟化而得。将水、间氨基酚和碳酸氢钠依次投入反应罐内，通入二氧化碳置换空气后，密闭升温至110±1℃，罐内压力保持0.6-0.8MPa反应6h，冷却至-5℃，加亚硫酸钠，过滤，水洗，合并洗滤液供酸化用。滤饼为间氨基酚回收物，套用。将上述洗滤液升温至10-15℃，用30-40%硫酸中和至pH为6.4-7.0，加入适量的亚硫酸钠与硫化钠溶液，经树脂脱色后，于30℃用30-40%硫酸调节至pH为3- 3.5，放置，甩滤，水洗至硫酸根合格，甩干得对氨基水杨酸。从苯乙酸出发也可以合成得到对氨基水杨酸。先使苯乙酸在浓硫酸和浓硝酸中在60℃下硝化，然后倾入冰水中，过滤析出2,4-二硝基苯乙酸[643-43-6]。硝化产率95%。将得到的产物加入10倍甲醇中，均匀混合后，通入干燥的氯化氢，加热至沸，冷却后析出2,4-二硝基苯乙酸甲酯晶体[58605-12-2]。酯化产率为80%。将酯化物溶解于热甲醇中，加入亚硝酸丁酯，再加入甲醇钠，静置数小时直至完全析出深红色沉淀物，分离沉淀物得中间产物。将其溶于稀氢氧化钾溶液中，加入盐酸酸化，使呈酸性。逸出二氧化碳气体，析出4-硝基-2-羟基苯腈。产率为80%，将此腈化物与水、浓硫酸、冰醋酸混合加热至沸，即可析出4-硝基水杨酸[619-19-2]。将4-硝基水杨酸溶解于25%碳酸钠溶液中，加入硫酸亚铁水溶液，再加适量的碳酸钠溶液，加热至沸，分离析出铁盐。过滤，滤液用乙酸调至pH=3,4-氨基水杨酸则析出。再过滤干燥，即得产品。工业品对氨基水杨酸含量大于70%，氯化物小于50ppm，硫酸根小于500ppm。\u003C\u002Fp>\u003Cp>2.结构Ⅰ聚芳砜的制备　在反应釜中加入等摩尔比的二苯醚二磺酰氯和联苯，以硝基苯作为溶剂，三氯化铁为催化剂，在130℃反应20h左右，直到反应物特性黏度达到0.66dL\u002Fg以上时终止反应。物料倾入甲醇或丙酮中，捣碎，离析出固体树脂，经洗涤、干燥、造粒即得产品。聚合反应式如下：\u003C\u002Fp>\u003Cp>\u003C\u002Fp>\u003Cp>3.结构Ⅱ聚芳砜的制备　以双酚钠盐与4,4'-双(4-氯苯基磺酰基)联苯为原料，用环丁砜作溶剂，于220℃缩聚而成。缩聚反应可采用两步法，即先制成双酚钠盐后再缩聚。也可采用一步法，即将等摩尔比的双酚S、4,4'-双(4-氯苯基磺酰基)联苯及一定量的环丁砜溶剂和脱水剂二甲苯置于反应釜中，加热熔解，在低于80℃下加NaOH（2倍摩尔双酚S），然后升温脱水，再蒸出二甲苯，将釜温升至220℃进行缩聚反应。当物料达到规定黏度时，加入一定量环丁砜稀释之，降温，停止反应，离析出聚合物，经水煮、过滤、干燥得粉状聚芳砜。\u003Cbr \u002F>\u003C\u002Fp>","\u003Ctd>\n\n\u003Ca href=\"\u002Fen\u002Fcas\u002F65-49-6_1150743.html#MSDSDiv\">对氨基水杨酸MSDS英文版\u003C\u002Fa>\n\n\u003C\u002Ftd>","2026-08-21T07:51:12.859463Z",false,[388,394,400,406,412,418],{"slug":389,"cid":390,"name":391,"nameZh":392,"cas":393},"785897049336844288","J-876682-7","2-(tert-Butylamino)acetic acid","N-叔丁基甘氨酸","58482-93-2",{"slug":395,"cid":396,"name":397,"nameZh":398,"cas":399},"785882405830397952","J-3601-0","3-Bromopropanoic acid","3-溴丙酸","590-92-1",{"slug":401,"cid":402,"name":403,"nameZh":404,"cas":405},"785888360316014592","J-1339697-8","Glycocyamine hydrochloride","胍基乙酸盐酸盐","14901-20-3",{"slug":407,"cid":408,"name":409,"nameZh":410,"cas":411},"850039998064365568","J-1032735-1","Propanediamide, 2-​amino-​, hydrochloride (1:1)","2-氨基丙二酰胺一盐酸盐","57471-66-6",{"slug":413,"cid":414,"name":415,"nameZh":416,"cas":417},"785882801982410752","J-1956063-0","L-Valine hydrochloride","L-缬氨酸盐酸盐","17498-50-9",{"slug":419,"cid":420,"name":421,"nameZh":422,"cas":423},"850034308251914240","J-1032725-0","N,N,N,N-tetramethylethane-1,2-diamine","N,N,N,N-四甲基乙二胺盐酸盐","7677-21-6",1792678512256,"zh-CN",[]]