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闪点（ºC）：未确定\n9. 比旋光度（º）：未确定\n10. 自燃点或引燃温度（ºC）：未确定\n11. 蒸气压（kPa,25ºC）：未确定\n12. 饱和蒸气压（kPa,60ºC）：未确定\n13. 燃烧热（KJ\u002Fmol）：未确定\n14. 临界温度（ºC）：未确定\n15. 临界压力（KPa）：未确定\n16. 油水（辛醇\u002F水）分配系数的对数值：未确定\n17. 爆炸上限（%,V\u002FV）：未确定\n18. 爆炸下限（%,V\u002FV）：未确定\n19. 溶解性：不溶于水、乙酸、乙醇、吡啶、二甲苯、甲苯，微溶于氯仿 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VAT:17.0%. Tax rebate rate:13.0%. . MFN tariff:6.5%. General tariff:20.0%",[312,315,318,321,324],{"key":313,"value":314},"危害码 (欧洲)","Xi",{"key":316,"value":317},"风险声明 (欧洲)","R20\u002F21\u002F22",{"key":319,"value":320},"安全声明 (欧洲)","22-36\u002F37\u002F39",{"key":322,"value":323},"RTECS号","CB8761100",{"key":300,"value":325},"3204170000","\u003Ctd>\n\n\u003Cp>\u003Cstrong>颜料蓝60毒理学数据:\u003C\u002Fstrong>\u003C\u002Fp>\n\u003Cp>\u003C\u002Fp>\u003Cp>1、急性毒性\u003C\u002Fp>\n\u003Cp>大鼠口径LD:2 mg\u002Fkg；大鼠气管LD50: 250 mg\u002Fkg；\u003C\u002Fp>\n\u003Cp>\u003C\u002Fp>\n\u003Cp>\u003Ca href=\"\u002Fen\u002Fcas\u002F81-77-6_401872.html#duXinDiv\">颜料蓝60毒性英文版\u003C\u002Fa>\u003C\u002Fp>\n\n\u003C\u002Ftd>","\u003Cp>方法 1：熔融法。\u003Cbr \u002F>以 2-氨基蒽醌为原料，经与温合碱碱熔后，用保险粉溶液精制得产物。或以 2-氨基蒽醌为原料，二甲亚砜为溶剂，与氢氧化钾进行碱熔反应，再经保险粉溶液精制后得产物。。\u003Cbr \u002F>在缩合锅中加入无水混合碱 595kg (氢氧化钾占 68%)，加热熔融后，加入 131kg 乙酸钠 (98%)、1.5kg 油酸 (工业品)。关闭缩合锅，加热至 185-190℃，同时用氮气驱赶空气，使反应液处于氮气保护下，于 30min 内加入 263kg 2-氨基蒽醌，控制温度不超过 215℃，加毕保温 1h，再加入 25kg 亚硝酸钠 (98%)，控制温度不超过 230℃，约 2h 内加完。继续搅拌 20min，完成碱熔反应。\u003Cbr \u002F>在精制锅中放入 5000L 水，通入氮气驱赶空气，放入碱熔物料，搅拌 2h；降温至 51℃左右，加入 110kg 保险粉，慢速搅拌，降温至 45℃时，结晶析出。过滤，滤饼用保险粉水溶液洗涤 (洗涤水由 20L 液碱、20kg 保险粉、5000L 水配制而成)，再用 45℃温水洗至滤液呈微蓝，抽干，得染料隐色体湿料。\u003Cbr \u002F>在打浆机中加入染料隐色体湿料，适量水打浆，并通入空气于 60℃氧化 6h 后，加入扩散剂 NNO 150kg 进行砂磨，喷雾干燥得成品。每批约 138kg (100%)。\u003C\u002Fp>\u003Cp>方法 2：溶剂法。\u003Cbr \u002F>在缩合锅中加入 15L 二甲亚砜、6.802kg 2-氨基蒽醌，于 1h 左右升温至 132℃，待 2-氨基蒽醌基本溶解，继续升温至 130-150℃维持 30min，使其完全溶解。此时停止加热，通入空气，温度约下降至 128℃，于 10min 内加入 4.4L 氢氧化钾溶液 (39.8%)。并继续通入空气，于 (125±2)℃保温反应 4h。然后加水 20L，物料温度降至 80℃左右过滤，用 50-60℃的水 40L 洗缩合锅，并用其洗滤饼，抽干。\u003Cbr \u002F>在精制锅中加入 380L 水，上述滤饼打浆 1h，加碱 27kg (43%氢氧化钠)，升温至 56-57℃，加入 5.44kg 保险粉 (85%)，保持温度 20min，再于 40min 内降温至 52℃，结晶析出，过滤，滤饼用 50℃左右洗涤水 [410L 水、5.8kg 氢氧化钠 (43%)、0.82kg 保险粉 (85%) 配制] 洗涤，再用清水洗涤抽干。\u003Cbr \u002F>在酸化锅中加水 100L，加入精制滤饼，打浆 2h，加水调体积至 200L，加硫酸调 pH 值为 2-3 (约用 12.34%的硫酸 10kg)。搅拌 20min 过滤，用水洗至中性，吹干。进行砂磨即得成品。\u003C\u002Fp>","\u003Ctd>\n\n\u003Ca href=\"\u002Fen\u002Fcas\u002F81-77-6_401872.html#MSDSDiv\">颜料蓝60MSDS英文版\u003C\u002Fa>\n\n\u003C\u002Ftd>","2026-08-21T07:51:12.859463Z",false,[332,338,344,349,355,361],{"slug":333,"cid":334,"name":335,"nameZh":336,"cas":337},"785875705589141504","J-10742-4","Neocuproine hemihydrate","新亚铜试剂半水合物","34302-69-7",{"slug":339,"cid":340,"name":341,"nameZh":342,"cas":343},"785898367673700352","J-1988074-7","Pantoprazole Sodium Sesquihydrate","泮托拉唑钠倍半水合物","164579-32-2",{"slug":345,"cid":346,"name":347,"nameZh":347,"cas":348},"785947418393841664","J-1874835-6","((Perfluorohexyl)ethyl)-2-chloropropenoate","96383-55-0",{"slug":350,"cid":351,"name":352,"nameZh":353,"cas":354},"785882335940710400","J-3147-5","Pigment Red 57:1","颜料红57:1","5281-04-9",{"slug":356,"cid":357,"name":358,"nameZh":359,"cas":360},"785891221192052736","J-1095551-6","Sudan Black B","苏丹黑B","4197-25-5",{"slug":362,"cid":363,"name":364,"nameZh":365,"cas":366},"785876430910132224","J-1352432-0","Carbasalate calcium","卡巴匹林钙","93803-83-9",1792671136822,"zh-CN",[]]